Make sure you get a decent test kit as well, it sounds like yours was off quite a bit. I like to use Elos, they are pretty precise. Also, make sure that you are testing at around the same time every day, especially if you start dosing. I would test first, then add your 2 part additive, this will allow you to determine about how much Alk your corals are using daily and make it easier to titrate the dose of additive to attain your target Alk and Ca.